Intergranular corrosion tests we, at applied technical services, offer intergranular corrosion testing to ensure the structural integrity of the tested metal remains satisfactory during the service life of metals and alloys. Metals and alloys, like other elements, have microstructures that can be described as grains. When a material such as stainless steel becomes susceptible to igc, it creates a weakness that then cracks. Mar 28, 2016 intergranular corrosion of an alloy may be caused by impurities at the grain boundaries enrichment of one of the alloying elements depletion of one of the elements that affects its corrosion resistance in grain boundary areas. Susceptibility to the intergranular corrosion of alloy 800. Intergranular corrosion tests igc two test methods namely a modified astm a262 25 and a modified double loop electrochemical potentiokinetic reactivation dlerp test was employed to determine susceptibility to igc. The test methods outlined in astm a262 have been developed to detect susceptibility to intergranular attack in austenitic stainless steels.
Feb 06, 2011 intergranular corrosion igc microstructure of metals and alloys is made up of grains separa ted by grain boundaries intergranular corrosion is a localized attack along the grain bo undaries, or immediately adjacent to grain boundaries, while the bulk of t he grains remain largely unaffected igc is associated. Abdel salam hamdy makhlouf, in intelligent coatings for corrosion control, 2015. Jul 21, 2017 download corrosion intergranular astm a262. Pdf determination of the susceptibility of austenitic stainless steel x5crni1810 to intergranular corrosion igc is performed by measuring the. Scully 1 david taylor naval ship research and development center, marine corrosion branch, bethesda, maryland 20084. An namlt value of more than 30 gcm 2 of surface is necessary before an alloy has become sensitised to intergranular corrosion or cracking. Standard practices for detecting susceptibility to.
Biddle 3 1arv offshore, 19962 landco building, vipavadeerangsit road samsaennai, phayathai, bangkok 10400, thailand. Intergranular corrosion igc, also known as intergranular attack iga, is a form of corrosion where the boundaries of crystallites of the material are more susceptible to corrosion than their insides. Pdf corrosion intergranular astm a262 free download pdf. Intergranular corrosion, dlepr test method, austenitic stainless. The corrosion rate obtained by this test has uniform and intergranular corrosion components. Ferrite stainless steels can also be affected by intergranular corrosion, but sensitization temperatures are different. Intergranular corrosion testing for cast, bar and forge materials ogmetengr materials 6 sep 14 11. Intergranular corrosion test igc per astm a262 at tcr engineering services, several methods exist for the testing of intergranular corrosion.
It was considered that igc was caused by the existence of precipitatefree zones pfzs because pfzs. The inchpound equivalents are in parentheses and may be. Strauss, huey and streicher are the common test methods. The intergranular corrosion igc behavior of 6061 aluminum alloy extrusions was investigated. Intergranular corrosion igc or intergranular attack iga, is an efficient test for screening a materials corrosion resistance under certain conditions.
Intergranular corrosion is the destruction of metal at the grain boundaries, usually on a microscopic scale. Listed below please find some of the most relevant regulations, codes and standards related to corrosion testing. Intergranular corrosion tests are primarily designed to detect carbide precipitates on grain boundaries. Jul 25, 2017 intergranular corrosion forms along the grain structure of metal.
Intergranular corrosion igc microstructure of metals and alloys is made up of grains separa ted by grain boundaries intergranular corrosion is a localized attack along the grain bo undaries, or immediately adjacent to grain boundaries, while the. The test method used to evaluate susceptibility to intergranular corrosion depends on alloy type. There are a number of recognised tests when it comes to the intergranular corrosion testing of corrosion resistant alloys cra. Intergranuler corrosion takes place due to higher rate of corrosion of grain boundary area of. Jul 17, 2017 intergranular corrosion can wreak havoc on steel sections. The iso 11846 method b is one of the most frequently used corrosion tests to investigate the intergranular corrosion susceptibility of al. Note 1see appendix x1 for information regarding test selection. Intergranular corrosion testing of austenitic stainless steels in nitric. Astm a test, intergranular corrosion, igc, astm a practice, testing, india download as pdf file. Cu alloys and involves the sample immersion in an aqueous solution containing 30 gl nacl and 10 mll concentrated hcl for 24 h. Choosing an intergranular corrosion test method since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility. Intergranular corrosion testing of 6000 aluminum alloys. All materials, are accompanied with mill test reports, and on customer requests, we can also offer additional test report. Detecting susceptibility to intergranular attack in austenitic stainless steels.
What is astm a262 intergranular corrosion test igc china. This is a corrosion type that attacks the boundaries of the metal crystallites, as opposed to attacking the surface of the metal. Material cracking in service is clearly undesirable. However, little igc occurred at the center plane of the extrusion thickness. Intergranular cracking or crazing is evidence of susceptibility. It is often caused by improper processing of the metal during manufacture or improper heat. Astm a practice free download as excel spreadsheet. Intergranular attack susceptibility for nickel alloys.
Intergranular corrosion igc testing is the only corrosion test performed as a standardized predelivery test. Intergranular corrosion igc, also known as intergranular attack iga, is a form of corrosion where the boundaries of crystallites of the material are. Corrosion intergranular astm a262 july 21, 2017 author. The level of sensitisation to intergranular corrosion of 5xxx series alloys fabricated sheet, plate or extrusion can be easily determined by measurement of the mass loss after exposure to nitric acid namlt test in accordance with astm g6704. Determination of resistance to intergranular corrosion of stainless steels part 2. These practices include five intergranular corrosion tests, namely. Intergranular corrosion igc testing services element. Webcorr provides corrosion consultancy services, corrosion expert witness and corrosion short courses for inhouse training, online and distance learning.
In the presence of tensile strength, cracking may occur along grain boundaries and this type of corrosion is frequently called interranular stress corrosion cracking igscc or simply intergranular corrosion cracking. Aug 03, 2019 the oxalic acid test is commonly used before the strauss test to determine if a sample is susceptible. Intergranular corrosion acceptance criteria clarification. Astm a262 intergranular corrosion test igc intergranular corrosion is sometimes also called intercrystalline corrosion or interdendritic corrosion. Intergranular corrosion can also be referred to as intergranular attack under a condition known as grain boundary depletion.
Astm a262 intergranular corrosion testing and analysis. Intergranular corrosion an overview sciencedirect topics. Intergranular corrosion tests igc two test methods namely a modified astm a262 and a modified double loop electrochemical potentiokinetic reactivation dlerp test were employed to determine the susceptibility to igc. Grainboundary chemistry and intergranular corrosion in. Choosing the correct method s rely on a complete understanding of your material and processes, as well as the. The test evaluates the resistance of extralowcarbon steels to sensitization and intergranular attack from welding or heat treatment processes. George corrosion igc by using various tests speci ed by astm. An electrochemical test for detecting the intergranular corrosion susceptibility of a duplex stainless steel j.
Duplex stainless steel welds and their susceptibility to. Intergranular corrosion igc refers to corrosion in between crystals or grains. This form of corrosion is usually associated with chemical segregation effects impurities have a tendency to be enriched at grain boundaries or specific phases. Modified astm a262 standard practices ecoppercopper sulfate, sulfuric acid test for detecting susceptibility to. Table 1 application of evaluation tests for detecting susceptibility to intergranular attack in austenitic stainless steels note 1for each corrosion test, the types of susceptibility to intergranular attack detected are given along with the grades of stainless steels in which they may be found. Corrosion, stainless steel, steel, building materials, sets of chemical elements. Duplex stainless steel welds and their susceptibility to intergranular corrosion b. Small amounts of iron in aluminum, wherein solubility of iron is low, have been shown to segregate in the grain. Localized attack adjacent to grain boundaries with relatively little corrosion of grains.
Using a variety of methods, including astm a262, astm g28 and astm a763, we can provide critical data about the metals corrosion resistance to prevent failures in the field. Determination of susceptibility to intergranular corrosion and. Determination of resistance to intergranular corrosion of ferritic, austenitic and ferritic. So could you please advise if this x20 magnification is a realistic test on a test specimen which is solution for 120hrs with a acid solution. Astm a262 intergranular corrosion testing of stainless steels.
Pdf intergranular corrosion in a martensitic stainless. Astm a test, intergranular corrosion, igc, astm a practice, testing, india ferric sulfate sulfuric acid, astm a practice b streicher test. Two test methods namely a modified astm a262 and a modified double loop electrochemical potentiokinetic. Cihal presented a study 20, which was a continuation of an earlier study dealing with electrochemical determination of sensitivity to intercrystalline corrosion of stainless steel. Astm a is the specification which governs five practices used to determine if the.
Intergranular corrosion facts and how to reduce the risk. Intergranular corrosion tests applied technical services. This situation can happen in otherwise corrosionresistant alloys, when the grain. The astm a262 testing specification contains five unique intergranular corrosion tests. Most alloys are susceptible to intergranular corrosion, also known as intergranular attack iga, when exposed to specific environments. To conduct these tests, w e carefully choose a method w hich is suitable for the steel grade and grain boundary composition to be tested.
This standard specifies the method of the determination of resistance to intergranular corrosion in austenitic and ferriticaustenitic duplex stainless steels. However, although some tests also claim to detect intermetallic phases, inter granular corrosion tests should not be relied on for this, as the response of cras to the test solutions vary widely. Intergranular corrosion can wreak havoc on steel sections. Intergranular corrosion was artificially induced in the face sheets of a series of cold plate specimens using an electrochemical process. Astm a262 is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion. Intergranular corrosion forms along the grain structure of metal.
This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. After the igc test in accordance with isodis 11846 method b, heavy igc was observed at the surface of the extrusion. Intergranular corrosion in a martensitic stainless steel detected by electrochemical tests article pdf available in corrosion houston tx 558. Pdf intergranular corrosion of aisi 316l steel milan. All materials stocked and supplied by metline industries pass the igc test.
Pdf assessment of intergranular corrosion in aisi type 316l. May 08, 2017 intergranular corrosion igc, also known as intergranular attack iga, is a form of corrosion where the boundaries of crystallites of the material are more susceptible to corrosion than their. A highly magnified crosssection can show the granular structure with a clearly defined boundary that chemically differs from the grain. Intergranular corrosion is an attack that occurs at the grain boundaries of a metal or alloy due to the precipitation of secondary phase. The possibility of using eddy current testing ect to detect sensitisation and igc was also assessed. In hot strong nitric acid solutions, stainless steels exhibit intergranular corrosion. Intergranular corrosion test igc per astm a at tcr engineering services, several methods exist for the testing of intergranular corrosion. Intergranular corrosion is sometimes also called intercrystalline corrosion or interdendritic corrosion. It is form of surface corrosion preferentially along the grain boundaries of metal. Intergranular corrosion occurs when the boundaries of metal crystallites or grains are attacked rather the surface of the metal. Alloy 22 is a nicrmo alloy nickelchromiummolybdenum and is one of the most versatile corrosion resistant alloys used in industry today. Intergranular corrosion testing for cast, bar and forge.
The samples are boiled in a cucopper sulfate mixture for 15 hours and then bent 180 over an equal diameter bend. Determination of susceptibility to intergranular corrosion. This situation can happen in otherwise corrosion resistant alloys, when the grain. Here we take a look at what causes it, and how to protect your steel. Intergranular corrosion coupon tested in accordance with astm. Some of the cold plate specimens were separated for destructive characterization of the extent of corrosion produced by the electrochemical process and to insure the induced corrosion was intergranular. But the test report obtained shows that there is a 0. The time and temperature required to produce susceptibility to intergranular attack iga is dependent on alloy composition, particularly the carbon content. Presently, the most widely used susceptibility test for intergranular corrosion of hastelloy alloy c276 is the ferric sulfatesulfuric acid test. The best known example of metallurgical effect on corrosion. Effect of grain boundary characteristics on intergranular. In the presence of tensile stress, cracking may occur along grain boundaries and this type of corrosion is frequently called interranular stress corrosion cracking igscc or simply. Corrosion rates are often measured from immersion testing of specimens.
There are various ways to test intergranular corrosion. Ferritic,austenitic and ferriticaustenitic duplex stainless steels corrosion test in media containing sulfuric acid. The oxalic acid etch test is rapid and nondestructive, but not quantitative. All materials, are accompanied with mill test reports, and on customer requests, we can also offer additional test report for igc test, from certified nabl approved laboratories. Intergranular corrosion acceptance criteria clarification hsemus petroleum. Both types of corrosion can result in loss of structural integrity of the affected metal and. The oxalic acid test is commonly used before the strauss test to determine if a sample is susceptible. Astm a 262 test, intergranular corrosion, igc, astm a262.
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